Difference between revisions of "Gas chromatography"

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== Description ==
 
== Description ==
  
An analytical technique for the qualitative and quantitative analysis of organic materials with boiling points below 550 C. Compounds with higher boiling points can be analyzed after chemical modifications, such as silylation. Gas chromatographs with mass spectrometer detectors can provide positive identification of compounds at the low parts per billion level. The sample, a gas or volatilized liquid, is injected through a port into a flowing stream of inert carrier gas such as helium, argon or nitrogen. The samples and carrier gas pass through a column which contains a stationary phase that separates the sample components through a gas-liquid partitioning process. The separated components are flushed sequentially from the column to a detector. Available detectors are flame ionization (FID), thermal conductivity (TCD), electron capture (ECD) and mass spectrometry (MS). The elapsed time from injection to detection is defined as the retention time for an individual species. Identification and quantification of the sample's components are achieved by comparison of their retention times and peak areas to those of reference standards analyzed under the same conditions.
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An analytical technique for the qualitative and quantitative analysis of materials. Gas chromatographs (GCs) are generally used to detect individual components in a mixture. The sample, a gas or volatilized liquid, is injected through a port into a flowing stream of inert carrier gas such as [[helium]], [[argon]] or [[nitrogen]]. The sample and carrier gas pass through a column which contains a stationary phase that separates the individual sample components viah a gas-liquid adsorption/desorption partitioning process. The separated components are flushed sequentially from the column to a detector. Available detectors are flame ionization (FID), thermal conductivity (TCD), electron capture (ECD) and mass spectrometry (MS). The elapsed time from injection to detection is defined by the retention time for an individual species. Identification and quantification of the sample's components are achieved by comparison of their retention times and peak areas to those of reference standards analyzed under the same conditions. Gas chromatographs with mass spectrometer detectors can provide positive identification of compounds at the low parts per billion level. Compounds with boiling points higher 550 C can be analyzed after chemical modifications, such as silylation.
  
 
== Synonyms and Related Terms ==
 
== Synonyms and Related Terms ==
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==Resources and Citations==
 
==Resources and Citations==
 
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* Wikipedia: [https://en.wikipedia.org/wiki/Gas_chromatography Gas Chromatograph] Accessed June 2023
 
* http://www.nga.gov/resources/scienceresearch/glossary.shtm
 
* http://www.nga.gov/resources/scienceresearch/glossary.shtm
 
 
* http://www.c2rmf.fr/homes/home_id21988_u1l2.htm
 
* http://www.c2rmf.fr/homes/home_id21988_u1l2.htm
 
 
* Walter Hopwood, Submitted information
 
* Walter Hopwood, Submitted information
  

Revision as of 12:16, 19 June 2023

Gas chromatograph

Description

An analytical technique for the qualitative and quantitative analysis of materials. Gas chromatographs (GCs) are generally used to detect individual components in a mixture. The sample, a gas or volatilized liquid, is injected through a port into a flowing stream of inert carrier gas such as Helium, Argon or Nitrogen. The sample and carrier gas pass through a column which contains a stationary phase that separates the individual sample components viah a gas-liquid adsorption/desorption partitioning process. The separated components are flushed sequentially from the column to a detector. Available detectors are flame ionization (FID), thermal conductivity (TCD), electron capture (ECD) and mass spectrometry (MS). The elapsed time from injection to detection is defined by the retention time for an individual species. Identification and quantification of the sample's components are achieved by comparison of their retention times and peak areas to those of reference standards analyzed under the same conditions. Gas chromatographs with mass spectrometer detectors can provide positive identification of compounds at the low parts per billion level. Compounds with boiling points higher 550 C can be analyzed after chemical modifications, such as silylation.

Synonyms and Related Terms

GC; Gaschromatographie (Deut.); chromatographie en phase gazeuse (Fr.);

Resources and Citations

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